CE 602 Discontinuous rectification

Distillation is used to separate liquid mixtures made up of individual liquids that are soluble in one another. Rectification refers to distillation in a counterflow. Ethanol/water is recommended as the liquid mixture for the CE 602. The liquid mixture is added to the evaporator (bottom) tank. The mixed vapour produced moves upwards in the column. The mixed vapour contains a higher concentration of the component with the lower boiling point (ethanol). It leaves the top of the column and is condensed using a condenser and a phase separation tank. Part of the condensate is collected in a tank as product while the rest is fed back into the column. Here, on its way downwards, it undergoes further heating and material exchange with the rising mixed vapour. This exchange causes the vapour phase to become richer in ethanol and the liquid phase to become richer in water. The liquid phase moves to the bottom where it is collected.

A sieve tray column and a packed column are available. The packed column is filled with Raschig rings. The reflux ratio is adjusted using valves.

Relevant measured values are recorded by sensors and displayed digitally on the switch cabinet. The evaporator is adjusted using a PID controller.

A large, clear process schematic on the switch cabinet makes it easy to assign all the process variables.

  • discontinuous rectification
  • comparison of packed and sieve tray column
  • vacuum mode possible
  • trays in sieve tray column removable

Columns: internal diameter: 50mm, height: 765mm
Water jet pump: final vacuum: approx. 200mbar
Tanks

  • top product: approx. 2000mL
  • phase separation: approx. 500mL

Evaporator

  • power output: 0…4kW
  • tank: approx. 10L

Heat transfer surface

  • top product condenser: approx. 0,04m2

Measuring ranges

  • temperature: 13 x 0…150°C
  • reflux ratio: 0…100%
  • cooling water flow rate: 30…320L/h
  • column differential pressure: 0…60mbar
  • system pressure gauge: -1…0,6bar

 

230V, 60Hz, 3 phases
400V, 50Hz, 3 phases

  1. discontinuous rectification with packed and sieve tray column
  2. interchangeable columns
  3. sieve tray column with 8 trays
  4. packed column with Raschig rings
  5. vacuum mode possible with water jet pump
  6. electrically heated evaporator
  7. tank for top product
  8. condenser and phase separation tank for top product
  9. all tanks made of DURAN glass and stainless steel
  10. adjustment of reflux ratio using valves
  11. 8 temperature measuring points per column
  • investigation and comparison of sieve tray and packed columns
    • in discontinuous mode
    • in vacuum mode
    • with different reflux ratios
    • with different numbers of trays
  • determination of concentration profiles
  • determination of temperature profiles
  • pressure loss over the column

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Product number

CE 602